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I am trying to save a file in LibreOffice Calc that is still usable in Microsoft Office Excel. Save as .xlms doesn't work.

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What do you mean by .xlms? I don't see that as a Save As option in LibreOffice 3.6. –  user25656 Feb 23 '13 at 1:20
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2 Answers

Open your spreadsheet in LibreOffice Calc. Navigate to File -> Save As.

Make sure you open the "File Type" menu:

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Then either select .xls or .xlsx depending on whether the version of Excel you are using is 2007 or newer:

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Click "Save" and there you go.

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Menu>File>Save As type ".xls".

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OP specified .xlms not .xls. Unless that's a typo! –  user25656 Feb 23 '13 at 2:52
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